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Please login to access the full content or check if you have access via Method 2: Titanium–Tetraene Complexes by Reaction of Trichloro(pentamethylcyclopentadienyl)titanium(IV) with Dipotassium ­Cyclooctatetraene

DOI: 10.1055/sos-SD-002-00576

Mikami, K.; Matsumoto, Y.; Shiono, T.Science of Synthesis, (20032461.

The mixed-sandwich compound [Ti(Cp*)(cot)] (7) is obtained from the reaction of [Ti(Cp*)Cl3] (6) with dipotassium cyclooctatetraene in tetrahydrofuran (Scheme 5).[‌57‌] The yield is lower than that obtained in the method using magnesium (Section

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