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13.29.1.3.5 Method 5: Alkylation and Acylation of 1,2,3,4-Thiatriazole-5-thiol

DOI: 10.1055/sos-SD-013-01396

Begtrup, M.Science of Synthesis, (200413847.

A number of 1,2,3,4-thiatriazole-5-thiols 10 (R1=alkyl or acyl) have been prepared by treatment of thiatriazole-5-thiol 19 with alkyl or acyl halides (Scheme 30).[‌83‌‌85‌] Alternative attack at N4 has been suggested,[‌59‌] but this has been shown not to occur.[‌24‌]

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