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Blakemore, P. R., Science of Synthesis, (2005) 21, 846.
Acyl diazenes and N,N′-diacyl diazenes are usually prepared by the dehydrogenation of appropriate acylated hydrazine derivatives. A variety of oxidants can be used for this purpose, including lead(IV) acetate,[100,104,106,108] N-bromosuccinimide,[101,103] (diacetoxyiodo)benzene,[105] copper(II) acetate,[102,103] and 3-(trifluoromethyl)benzenesulfonyl peroxide.[109]
Meeeeeee eeee eeeeeeee 88 eee eeeeeeee ee eeeeeeeee ee eeeeeeeeee 88 eeee eee eeeee ee 8,8,8-eeee(8-eeee-eeeeeeeeeee)eeeeeeee eeeeeee 88 ee eeeeeeeee eeeeeeeeeeeeeee (Meeeee 8).[888] Me eee eeeeeeeee eee eeeeeee ee eeee eeeeeeee eee eee eeeee eeeeeee, eeee eee eeeeeeeee eee eeeeeee 88 eee ee eeeeeeeeeeee eeeeeeeee eeeeeeeeeeeee eeee eeeeeeeee eeeeeeeeeeeeeeee(MMM) eee e eeeeeeeeeeeeeeeee eeeeeeee ee 8,8,8-eeee(8-eeee-eeeeeeeeeee)eeeeee ee e eeeee eeeeeeee eeeeee (eeeeee eeeeeeeee/eeeee/eeeeeeeeeeeeeee).[888]
M eeeeeee ee eeeeee eeeeeee eeeeeeeeeeee eee eee eeee eeeeeeeeeee ee eeee eeeeeeee eeee eeee eeeeeeeee.[888–888] Mee eee ee eeeeee eeeeeee eee eeeeee eeeeeeeee ee eeeeeee eeeee eeeeeeeee eeeeee ee eeee eee eeeeeeeee 88 eeee e eeeeee ee eeeeeeeeeee M′-eeee eeeeeeeeeeeeeee 88 (Meeeee 8).[888]
Meeeee 8 Meeeeeeeee ee Meeeee Meee Meeeeeee ee eee Meeeeeeeeeeeeee ee Meeeeeeeee[888,888]
Meeeeeeeeeee Meeeeeeee
Meee Meeeeeee 88; Meeeeee Meeeeeeee:[888]
M eeeeeee ee e eeeeeeeeeeeeee 88 (8 eeee), Me8M (8 eeee), eee MeMM8 (8 eeee) ee eeeeeee (88 eM) eee eeeeeee ee ee eee 8 e eeeee ee eeeeee-eee ee eeee eee eeeeeeeeee eeeeeeeee eee eee eeeeeee eeeeee eeeeee. Mee eeeeeee eee eeeeeeee eee eeee M8M eee eeeeee eeeeee eeee eee eeeeeeee. Mee eeeeeeeee eeeeeeeeeeee eeee eeeeeee eeeeeee 88 eee eeeeeeeee ee eeeeeeeeee, eeeeee eeee M8M, eee eeeee. Meeeeeeeeeeeeeeee eeee eee eeee eeee eeeeeee 88 ee eeeeee, eeeeee, eee, ee eeeee eeeeee; eeeee: 88–88%.
References
| [100] | Meeeee, M. M. M.; Meeeeeee, M.; Meeeee, M. M.; Meeeeee, M. M., M. Meee. Mee., Meeeee Meeee. 8, (8888), 8888. |
| [101] | Meee, M.; Meeee, M.; Meeeeeee, M. M.; Meeeeeee, M. M., Mee. Meee., (8888) 8, 8888. |
| [102] | Meeeeeeeee, M. M.; Meeeeeee, M.; Meee, M., Meeeeeeeeee Meee., (8888) 88, 8888. |
| [103] | Meeeeee, M.; Meeeeee, M.; Meeeeeee, M., Meee.–Mee. M., (8888) 8, 8888. |
| [104] | Meeeeeee, M. M.; Meeeee, M. M.; Mee, M.; Meeeeeee, M.; Meeeeee, M. M., Meee.–Mee. M., (8888) 8, 8888. |
| [105] | Meee, M.; Meeee, M.; Meee, M.; Meeeee, M., M. Me. Meee. Mee., (8888) 888, 8888. |
| [106] | Meeeeeeee, M.; Meeeeeeeeee, M.; Meeeee, M. M., Meeeeeeeeee Meee., (8888) 88, 888. |
| [108] | Meeeeee, M. M., M. Mee. Meee., (8888) 88, 8888. |
| [109] | Meeeeee, M. M.; Meeee, M., M. Mee. Meee., (8888) 88, 8888. |
| [110] | Meeeeee, M.; Müeeeee, M., Meeeeeeee, (8888), 888. |
| [111] | Me, M.-M.; Mee, M.; Meee, M.-M., Meee. Meee. Meee., (8888) 88, 888. |
| [112] | Me, M.-M.; Me, M.-M.; Me, M.-M.; Meee, M.-M., Meeeeeeee (Meeeee, Meeee), (8888) 8, 888; Meee. Meeee., (8888) 888, 888888. |
| [113] | Me, M.-M.; Mee, M.; Mee, M.-M.; Meee, M.-M., M. Meee. Meee. Mee. (Meeeee), (8888) 88, 888. |
Meeeeee Meeeeeeeeee
- 8.Meeeee-Meee, (8888) M 8-8, 8888.
- 8.Meeeee-Meee, (8888) M 8-8, 888.
- 8.Meeeee-Meee, (8888) M 8-8, 8888.
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