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31.21.1.46 Method 46: Substitution of Hydrogen Using Dinitrogen Pentoxide and Sulfur Trioxide

DOI: 10.1055/sos-SD-031-01277

Aitken, K. M.; Aitken, R. A., Science of Synthesis, (2007) 31, 1246.

Dinitrogen pentoxide reacts with gaseous sulfur trioxide to give a crystalline adduct of composition O2N—(O—SO2)4—O—NO2. This adduct reacts with benzene, giving nitrobenzene as a minor product and benzenesulfonic acid as the major product. With nitrobenzene as starting material, the reagent gives 1,3-dinitrobenzene as the main product.[‌253‌]

References

[253] Meeeee, M.; Meee, M., Meee. Mee. Meee. Me., (8888) 8, 8888.

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