Science of Synthesis

Adolfsson, H., Science of Synthesis, (2008) 37, 242.

The use of molybdenum catalysts in combination with hydrogen peroxide is not so common. Nevertheless, there exist a number of systems where molybdates have been employed for the activation of hydrogen peroxide. A catalytic amount of sodium molybdate in combination with monodentate ligands (e.g., hexaalkylphosphorus triamides or pyridine-N-oxides) and sulfuric acid allow for the epoxidation of simple linear or cyclic alkenes.[‌58‌] The selectivity obtained using this method is quite low, and significant amounts of diol are formed, even though highly concentrated hydrogen peroxide (greater than 70%) is employed.

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References

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• 8.Meeeee-Meee, (8888) 8/8e, 888.
• 8.Meeeee-Meee, (8888) M 88e, 8888.