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DOI:
10.1055/sos-SD-037-00438
Robina, I.; Vogel, P., Science of Synthesis, (2008) 37, 652.
The synthesis of 1,3-anhydro-2,4-O-benzylidene-d-glucitol 44 starts from 2,4-O-benzylidene-1,6-di-O-tosyl-d-glucitol (42) through regioselective generation of epoxide 43, followed by oxetane formation and epoxide ring opening. Final deprotection under acidic conditions gives the 1,3-anhydro-d-glucitol derivative 45 (Scheme 8).[42]
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References
[42] | Meeeeeee, M. M., Meeeeeeee. Mee., (8888) 888, 888. |