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41.7.2.1.1 Method 1: Synthesis from Diazoalkanes

DOI: 10.1055/sos-SD-041-00494

Kubik, S.Science of Synthesis, (201041517.

Reaction of diazomethane with N-[chloro(dimethylamino)methylene]-N-methylmethanaminium chloride leads to the formation of 2,2-bis(dimethylamino)ethenediazonium chloride (16) (Scheme 18).[‌128‌] This compound could not be obtained in crystalline form but was identified spectroscopically.

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