Science of Synthesis

Vil’, V. A.; Bityukov, O. V.; Terent’ev, A. O., Science of Synthesis Knowledge Updates, (2019) 3, 388.

The most widely reported methods for the synthesis of geminal bishydroperoxides involve the acid-catalyzed addition of hydrogen peroxide to acetals, enol ethers, or carbonyl compounds and ozonolysis of enol ethers or geminal disubstituted alkenes in the presence of hydrogen peroxide (‌Scheme 9‌).

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References