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38.11.4 Bis(1-hydroperoxyalkyl) Peroxides

DOI: 10.1055/sos-SD-138-00067

Vil, V. A.; Bityukov, O. V.; Terentev, A. O.Science of Synthesis Knowledge Updates, (20193419.

Bis(1-hydroperoxyalkyl) peroxides [1,1-bis(hydroperoxy)bis(alkyl)peroxides] can be synthesized from carbonyl compounds, acetals, or bishydroperoxides using hydrogen peroxide and various acids (Scheme 40). Substitution of a hydroxy group for a hydroperoxy group in 1-hydroperoxyalkyl 1-hydroxyalkyl peroxides also leads also to bis(1-hydroperoxyalkyl) peroxides (Scheme 40). Other miscellaneous approaches to bis(1-hydroperoxyalkyl) peroxides involve ozonolysis of enol ethers or alkenes and treatment of ethers with oxygen (not presented in Scheme 40).

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