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6.2.1 Fluidized Bed Electrode Systems

DOI: 10.1055/sos-SD-236-00125

Villani, E.; Inagi, S.Science of Synthesis: Electrochemistry in Organic Synthesis, (20211158.

The fluidized bed electrode (FBE) system first appeared in the late 1960s, when Goodridge and collaborators described an electrochemical method to perform uniform electrodeposition of metallic coatings on conducting and non-conducting particles, which form a fluidized bed electrode in a plating bath.[‌23‌] Later on, they also reported the use of the same technology for a variety of electrochemical reactions, such as the cathodic reduction of 3-nitrobenzene sulfonic acid,[‌24‌] or the electrolysis of seawater for the production of hypochlorite, or of bromide solution for the production of hypobromite, and for decarboxylation reactions.[‌25‌] FBE technology is also suited to electroorganic synthesis involving a gaseous reactant, for example propene, for the electrochemical production of 2-methyloxirane (propylene oxide) by reaction with a halogen generated in situ by the anodic oxidation of an alkali metal halide salt in aqueous solution.[‌26‌]

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