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2.5.1.2 Photocatalyst-Mediated C—H Functionalization

DOI: 10.1055/sos-SD-241-00086

Wang, X.; Lu, X.Science of Synthesis: DNA-Encoded Libraries, (20241243.

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Meeee Meeeeee Meeee (%) Mee
88 [‌88‌]
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88 [‌88‌]
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88 [‌88‌]
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88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
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Meeeee 88 Meeeeee-Meeee-Meeeeee MM Meeeeeeeee ee M-Meee Meeeeeee Meeeee[‌88‌]

Meeeeeeeeee 88

M8 M8 M8 M8 Me8 Meeee (%) Mee
M M M Me 8-eeeeeee 88 [‌88‌]
Me M (MM8)8 Me 88 [‌88‌]
Me M (MM8)8 Me 88 [‌88‌]
Me M MM8M(MM8)8 Me 88 [‌88‌]
Me M M Me 8-eeeeeee 88 [‌88‌]
Me M M Me Me 88 [‌88‌]
8-MeMM8M8 M M Me Me 88 [‌88‌]
8-M8MM8M8 M M Me Me 88 [‌88‌]
Me M (MM8)8 Me 88 [‌88‌]
(MM8)8 (MM8)8 Me 88 [‌88‌]
Me M (MM8)8 8-MM8MM8M8 88 [‌88‌]
M Me 8-MM8MM8M8 88 [‌88‌]
8-M8MM8M8 M MM8M(MM8)8 8-MMMM8M8 88 [‌88‌]
Me M MM8M(MM8)8 8-MMMM8M8 88 [‌88‌]
8-M8MM8M8 M (MM8)8 88 [‌88‌]
8-MeMM8M8 M (MM8)8 88 [‌88‌]
M (MM8)8 88 [‌88‌]

Meeeeeeeeee 88M

e M8 Me8 Meeee (%) Mee
8 M Me 88 [‌88‌]
8 MM8M 88 [‌88‌]

Meeeeeeeeee 88M

e M Me8 Meeee (%) Mee
8 MM8 Me 88 [‌88‌]
8 M 8-MMMM8M8 88 [‌88‌]

Meeeee 88 Meeeeeeeeeeee MM Meeeeeeee ee Meeeeeeee[‌88‌]

Meeeeeeeeee 88

M M8 M8 Me8 Meeee (%) Mee
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M M 88 [‌88‌]
M M Me 88 [‌88‌]
Me M M 88 [‌88‌]
Me M M 88 [‌88‌]
M M M 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
M Me M 88 [‌88‌]
M Me M 88 [‌88‌]
M M Me 88 [‌88‌]
M M Me 88 [‌88‌]
Me M M 88 [‌88‌]

Meeeeeeeeee 88M

Me8 Meeee (%) Mee
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]
88 [‌88‌]

Meeeeeeeeee 88M

Me8 Meeee (%) Mee
88 [‌88‌]
88 [‌88‌]

Meeeeeeeeee 88M

Me8 Meeee (%) Mee
88 [‌88‌]
88 [‌88‌]
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Meeee 8 Meeee-Meeeeeeeeeeeeee Meeeeeee ee MMM-Meeeee Meeeeeeeeeeeeeeeeeeeeee eeee Meeeeeeeeeee[‌88‌]

Meeeeeeee Meeeeee Meeee (%) Mee
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Meeeee 88 Meeeeee-Meeee-Meeeeeee MM Meeeeeeeeeee Meeee eee Meeeeeeeee Meeeeeeeee ee Meeee Meeeeee (MMMM) Meeeeeee[‌88‌]

Meeeeeeeeee 88

M8 M8 Meeee (%) Mee
M Me 88 [‌88‌]
M Me 88 [‌88‌]
M 8-eeeeeee 88 [‌88‌]
M 8-Mee 88 [‌88‌]
M 8-MeMM8M8 88 [‌88‌]
M 8-MMM8M8 88 [‌88‌]
M 8-MMM8M8 88 [‌88‌]
M 8-MMM8M8 88 [‌88‌]
M 8-MM8M8 88 [‌88‌]
M 8-MeM8M8 88 [‌88‌]
M 8-MeM8M8 88 [‌88‌]
M 8,8-M8M8M8 88 [‌88‌]
M 8-M8MM8M8 88 [‌88‌]
M 8-MeM8MM8M8 88 [‌88‌]
M 8-MM8MM8M8 88 [‌88‌]
Me Me 88 [‌88‌]
Me 8-MeMM8M8 88 [‌88‌]
Me 8-MMM8M8 88 [‌88‌]
Me 8-eeeeeee 88 [‌88‌]

Meeeeeeeeee 88M

M8 Meeee (%) Mee
Me 88 [‌88‌]
8-MeMM8M8 88 [‌88‌]
8-MMM8M8 88 [‌88‌]
8-eeeeeee 88 [‌88‌]

Meeeeeeeeee 88M

M8 Meeee (%) Mee
Me 88 [‌88‌]
8-MeMM8M8 88 [‌88‌]
8-MMM8M8 88 [‌88‌]
8-eeeeeee 88 [‌88‌]

Meeeeeeeeee 88M

M8 Meeee (%) Mee
Me 88 [‌88‌]
8-MeMM8M8 88 [‌88‌]
8-MMM8M8 88 [‌88‌]
8-MM8M8 88 [‌88‌]
8-M8MM8M8 88 [‌88‌]
8-MeM8MM8M8 88 [‌88‌]
8-eeeeeee 88 [‌88‌]
Me 88 [‌88‌]

Meeeeeeeeeee Meeeeeeee

Me-MMM M-(eeee-Meeeeeeeeeeeee)eeeeeeeeeee 88; Meeeeee Meeeeeeee:[‌88‌]

Me e eeeeeee ee MMMM (88 µM) eee eeM8M (88 µM) eeee eeeee e 8 M eeee ee eee Mee-eeeeeeeee eeeee ee MMMM (88 µM, 8888 eeeee) eee e 8 M eeee ee eeeeeeeeeeee ee MMMM (88 µM, 8888 eeeee) ee 8 °M. Meee, e 8 eM eeee ee MMM-eeeeee eeeeeeeeee ee eeM8M (88 µM, 8 eeeee) eee e 8 eM eeee ee [Me{eM(MM8)eee}8(eeeeee)}MM8 ee MMMM (88 µM, 8 eeeee) eeee eeeee. Mee eeeeeeeee eeee eee eeeeeeee eeeee M8 eee eeeeeeeeee eeee e eeee MMM (8–8 ee eeee eeee eee eeee) ee 88–88 °M eee 88 eee. Mee eeeeeeeee MMM-eeeeee eeeeeee eee eeeeeeee ee eeeeeee eeeeeeeeeeeee.

Me-MMM M-Meeeeeeeeeeeeee 88; Meeeeee Meeeeeeee:[‌88‌]

Me e 88-eeee eeeee eeee eeeee e 8 eM eeee ee eee MMM-eeeeee eeeeee ee eeM8M (88 µM, 8 eeeee), 8.8 M M8MMM8 ee eeM8M (8 µM, 888 eeeee), e 8.8 M eeee ee eee eeeeeeee eeeee ee MMMM (8 µM, 888 eeeee), 8.88 M [Me{eM(MM8)eee}8(eeeeee)]MM8 ee MMMM (8 µM, 8 eeeee), eee MMMM (88 µM) eeeeeeeeeeee. Mee eeeeeeeee eeeeeee eee eeeeeeee eee 88 e; eeee, eee eeeee eee eeeeeeeeeee ee e eeeeeeee ee eeeeeee eeeeeeeee eeeee M8 eee 8 e. Meeee eeee, eee eeeee eee eeeeeeeeee eeee e eeee MMM (Meeeeeee Meeeeeee Meeeeeeeeee Meeeeeeeee; λ ≈ 888ee, M = 88.8 M) eee 8 e eeeee M8. Mee eeeeeeee eeee eee eeeee eeeeee ee eee eeeeeeeeeee eeeeee eee ee. 8.8 ee. Mee eeeeeeeee MMM-eeeeee eeeeeee eee eeeeeeee ee eeeeeee eeeeeeeeeeeee.

Me-MMM Meeeeeeee 88; Meeeeee Meeeeeeee:[‌88‌]

Me ee Meeeeeeee eeee eee eeeee e 88 eM eeee ee eMe8MMe ee MMMM (8.8 µM, 8 eeeee), e 8 eM eeee ee eee-Me(eee)8 ee MMMM (8.8 µM, 8.8 eeeee), e 888 eM eeee ee eee eeeeeeee ee MMMM (88 µM, 888 eeeee), eee e 8 eM eeee ee eee MMM-eeeeeeee eeee eeeeee ee eeM8M (8 µM, 8.8 eeeee). Mee eeee eee eeeeee, eeeeeeee, eee eeeeeeeeee eee 8–88 eee eeee Meeeee MM 888 eeeee ee e eeeeeeee ee 8.8 eeeeee (eeeeee. 8 ee). Mee eeeeeee eee eeee eeeeeee eeee eeM8M (888 µM), eeeeeeee eeeeeee MeeeeMeeeee eeeeee eeeeee eee eeeeeeeeee eeeeee, eee eeeeeeeeeeee eeeeeeee ee MM/MM.

Me-MMM 8-Meee-8-(eeeeeeeeeee)-8,8,8,8-eeeeeeeeeeeeeeeeeeeeeee 88; Meeeeee Meeeeeeee:[‌88‌]

Me ee Meeeeeeee eeee eeee eeeee e 8 eM eeee ee eee MMM-eeeeee eeeeeeeeeeeeeeeeeeeeee ee eeM8M (88 µM, 8.8 eeeee), MeMM8 (88 µM), MeMM (88 µM), eee e 8 eM eeee ee [Me{eM(MM8)eee}8(eeeee)]MM8 ee MeMM (8 µM, 8 eeeee). Mee eeee eee eeeeee, eeeeeeee, eee eeeeeeeeee eee 8 e ee ee eeee 88-M eeee eeeee ee e eeeeeeee ee 8–8 ee. Meeee eeeeeeee, e 888 eM eeee ee eee eeeeeeeee eeeeee eeeeeeeeeeeeeeeeeeeeee ee eeM8M (8.8 µM) eee eeeee ee eee eeeeeee ee eeeeee eee eeeee eeeeeeee. Mee eeeeeeeee MMM-eeeeee eeeeeee eee eeeeeeee ee eeeeeee eeeeeeeeeeeee.

Me-MMM 8-(Meeeeeeeeeeee)-8M-eeeeeee 88; Meeeeee Meeeeeeee:[‌88‌]

Mee eeeee (Meeeeeeeee Meeeee-MM) eee eeeeeee eeee e eeeeeeeeeeeeeee eeee eee 8M MMM eeeeee/MeMM (8:8) eee eeeee eee 88 eee ee eeeee eee eeeee. Me e 8.8-eM Meeeeeeee eeee eee eeeee eee eeeeeee eeeee (888 µM) eee 8M MMM eeeeee (888 µM). Mee eeeeeeee eeee eeeeeeee, eee eeeee eeeeee eee eeee eeee, eee eee eeeeeeeeeee eee eeeeeeeee. Me eee eeeee eee eeee eeeee e 8 eM eeeee eeee ee eee MMM-eeeeee eeeeee ee eeM8M (8 µM, 8 eeeee) eee MMM eeeeee (888 µM). Mee eeeeeee eee eeeeeeee eee eeeeeeee ee eeeeeee eee 88 eee ee eeee eee MMM eeee eee eeeee. Meee, eee eeeeeee eee eeeeeeeeeee, eee eee eeeeeeeeeee eee eeeeeeeee. Mee eeeeeeeee eeeee eee eee eeeeee eeee eee MMMM (8 × 888 µM). Meee, eee eeeee eeeeeee eee eeeeeeeeeee ee e eeeeee eeee, eeeeeeee ee MMMM (888 µM) eee eee eeeeee eeeeeeeeee (8.8 eeee, 88 888 eeeee). Mee eeeeeeeee eeeeeee eee eeeeeeee eee eeeeeeeeee eeee e eeeeeeee eeeee eeeeee (88-M MMM, 888 ee MMM, ee 888 ee MMM) ee ee eee 88 e. Meee, eee eeeeeee eee eeeeeee eeee eeeeeeeeee MMM (8 × 888 µM), eeeeeeee, eee eeeeeeeeeee eee eee eeeeeeeeeee eee eeeeeeeee. Me eee eeeee eee eee eeeee MMM eeeeee (8 × 888 µM), eee eeeeeee eee eeeeeeee eee eeeeeeeeeee, eee eee eeeeeeeeeee eee eeeeeeeee. Meeeeee eeeeee [8 M MeMeM8, 88 eM Meee (eM 8.8), 88% MeMM; 888 µM] eee eeeee eee eee eeeeeee eee eeeeeeee eee eeeeeeee ee eeeeeee eee 88 eee; eeeee eeee, eee eeeeeee eee eeeeeeeeeee eee eee eeeeeeeeeee eee eeeeeeeee. Mee eeeeeee eee eeeeeeee eeee eee eeeeeeeee eeee ee eeeeeee eeeeeeeeeeeee.

References


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