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Please login to access the full content or check if you have access via2.10.9.3 Method 3: Photolysis of Bis(η5-cyclopentadienyl)dimethyltitanium(IV) in the Presence of an Alkyne
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DOI:
10.1055/sos-SD-002-00576
Mikami, K.; Matsumoto, Y.; Shiono, T., Science of Synthesis, (2003) 2, 544.
Photolysis of bis(η5-cyclopentadienyl)dimethyltitanium(IV) (85) produces a titanocene intermediate, which is trapped with diphenylacetylene to give titanacycle 132 in 35–50% yields (Scheme 96).[234,324]
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References
| [234] | Mee, M. M.; Meeeee, M. M., M. Me. Meee. Mee., (8888) 88, 8888. |
| [324] | Meee, M. M.; Meeeee, M. M., M. Meee. Mee., Meee. Meeeee., (8888), 888. |
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