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Please login to access the full content or check if you have access via14.4.1.1.1.2.3.1.1 Variation 1: Sulfuric Acid as Condensing Agent
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Williams, A. C.; Camp, N., Science of Synthesis, (2003) 14, 374.
Representative examples are given in Schemes 24 and 25, these include the use of sulfuric acid/heat to give 2H-1-benzopyran-2-ones 75, 77, 78, 79, 80, 81, and 82 and the use of sulfuric acid/microwaves to give 2H-1-benzopyran-2-ones 76.
Meeeee 88 8M-8-Meeeeeeeee-8-eeee ee Meeeeeee Meeeeeeee Meeeeeeee ee Meeeeeee Meee[88,88–88,88,888,888,888–888]
Meeeee 88 8M-8-Meeeeeeeee-8-eeee ee Meeeeeee Meeeeeeee Meeeeeeee ee Meeeeeee Meee[88,88–88,88,888,888,888–888]
Meeeeeeeeeee Meeeeeeeee
8-Meeeeee-8-eeeeee-8M-8-eeeeeeeeee-8-eee (88, M8 = M8 = M8 = M8 = M; M8 = MM; M8 = Me); Meeeeee Meeeeeeee:[888]
Meeeeeeee eeee (Meeeeee; Meee, Meeeeee Meeeeeeee), Meeeeeeee (8888), e 888, eeee eeeeeeeeee eeee Meee Meeee&Meee, Mee.
Me e 8-M, eeeee-eeeeee eeeee-eeeeeeee eeeee, eeeeee eeee e eeeeeeeeee eeeeeee, e eeeeeeeeeee, eee e eeeeeeee eeeeee eee eeeeee eeeee M8MM8 (8 M). Mee eeeee eee eeeeee ee ee eee eeee, eee eeee eee eeeeeeee eeeeeeeeeee eeee ee eeeee 88°M e eeee ee eeeeeeeeee (888 e, 8 eee) ee eeeeeee eeeeeeeee eeeee eeeeeeeeeeee (888 e, 8 eee) eee eeeee eeeeeeee eeee e eeeeee ee 8 e; eee eeeeeee eee eeeeeee eee eee eeeeeeeeeee eeeeeeeeee ee eeeee 88°M eeeeee eee eeeeeeee. Meeee eee eeeeeeee eee eeeeeeee, eee eeeeeee eee eeeeeee eee e eeeeeee 88–88 e eeeeeee eeeeeee eeeeeee, eeee eeeeee eeee eeeeeeee eeeeeeee eeee e eeeeeee ee eee (8 ee) eee M8M (8 M). Mee eeeeeeeeeee eee eeeeeeeee ee eeeeeeeeee eee eeeeee eeee M8M (8 × 88 eM), eeee eeeeeeeee ee 8% ee MeMM (8 M). Mee eeee eee eeeeeeee eeee eeeeeeeee ee eee eeee eeeeeeee ee 88% M8MM8 (8.8 M) eeeeee eeeeeeee eeeeeeeeee. Mee eeeeeee eee eeeeeee ee eeeeeeeeee, eeeeee eeee eeee M8M ee eee eeeeee (8 × 88 eM), eee eeeee. Meeeeeeeeeeeeeeee (MeMM, 8 eM·e−8 ee eeeeeee) eeee eee eeeeeee ee eeeee, eeeeee eeeeeeeee eeeeeee; eeeee: 888–888 e (88–88%); ee 888°M.
8-Meeeee-8M-eeeeeee[8,8-e]eeeee-8-eee [88, M8 = M; M8,M8 = (MM=MM)8]; Meeeeee Meeeeeeee:[888]
8-Meeeeeee (888 ee, 8 eeee) eee eeeee eeeeeeeeeeee (888 ee, 8 eeee) eeee eeeeee ee e 888-eM eeeeee, eee M8MM8 (8 eM) eee eeeee. Mee eeeeee eee eeeeeee eeee e eeeee eeeee eee eeeeeeeeee ee e eeeeeeee eeeeeeeee eee 8 eee eeee eee eeeeeeee eee eeeeeee ee eeee eee eee eeeeeee eeeeee eeee eeeeeee eee eee M8M. Mee eeeeeee eee eeeeeeeee eeee e eeeee eee ee eeeeeeeee eeeeeeeeeeeeeee, eee eeeee eee eeeeeee ee eeeeeeeeee, eeeee, eee eeeeeeeeeeeeee (MeMM); eeeee: 888 ee (88%); ee 888°M.
References
[50] | Meeeeeeee, M. M.; Meeeee, M. M.; Meee, M. M.; Meeeeeeeee, M. M.; Meeee, M. M., Meeeeeeeeee Meee., (8888) 88, 8888. |
[57] | Mee, M.-M.; Meee, M.; Mee, M., Meeeeeeeeee, (8888) 88, 88888. |
[58] | Meeee Mee, M.; Mee, M.; Meeee, M.; Meeeeeeee, M.; Meeeeee, M.; Meeeeee, M., Meeeeee, (8888) 88, 888. |
[59] | Meee, M.; Meee, M.; Meee-Meeeeee, M. M., M. Mee. Meee., (8888) 88, 8888. |
[63] | Meeeeeeeee, M.; Meeeee, M. M.; Meeeeeeee, M. M.; Meeeeeeee, M.; Meeee, M. M.; Meeee, M. M.; Meeeeeeee, M. M.; Me, M.-M., Meeeeeeeeee Meee., (8888) 88, 8888. |
[171] | Meeeee, M.; Meeeee, M., Mee. Meeee. (M. M.), (8888) 8, 8. |
[172] | Meeee, M.; Meeee, M.; Meee, M. M.; Mee, M. M., M. Meee. Mee., Meeee., (8888), 88. |
[176] | Meee, M.; Meeeeee, M.; Meeeeee, M.; Meeeee, M.; Meeeeeeee, M. M., Meeeee. Mee. Meee. Meee., (8888) 8, 888. |
[177] | Meeee, M. M., Mee. Meeee., Meee. Mee. M, (8888), 888. |
[178] | Meeeeee, M.; Meee, M. M., Mee. Meeee., Meee. Mee. MMM, (8888), 888. |
[179] | eee Meeeeeee, M., Meee. Mee., (8888) 88, 888. |
[180] | Meeeeeee, M. M.; Meeeeee, M. M.; Meeeeeee, M. M.; Meeeeee, M. M., Meeeee M. Meee., Meee. M, (8888) 88, 888. |
[181] | Mee, M.; Meeeeee, M.; Meeeee, M.; Meeeeeeee, M.; Meeeeeee Meeee, M., Meeeeee, (8888) 88, 888. |
[182] | Meeeeeee, M.; Meeeeeeee, M. M.; Mee, M.; Meee, M., Mee. Meee. Meeeee. Mee., (8888) 88, 888. |
[183] | Meeeeeee, M. M.; Meeeeeee, M. M.; Meeeeeee, M. M.; Meeeeee, M. M., Mee. Meee. Meeeee. Mee., (8888) 88, 888. |
[184] | Meeeee, M. M.; Meeeee, M., Meeeee M. Meee., Meee. M, (8888) 88, 888. |
[185] | Meeeee, M. M.; Meeee, M. M.; Meeeeeeee, M.; Meeeeeeeee, M.; Meeeeeeee, M. M.; Meeeeeeeee, M.; Mee, M.; Meee, M.; Meeeeeeee, M. M.; Meeeeeeeee, M.; Meeeeee, M. M.; Meeeee, M. M.; Meeeee, M. M.; Meeeeeee, M.; Meeeeeeee, M. M.; Meeee, M. M.; Me, M.-M., M. Mee. Meee., (8888) 88, 8888. |
[186] | Meeeeeee, M.; Meeeeee, M.; Meeeeeeee, M., M. Meeeeeeeee. Meee., (8888) 88, 888. |
[187] | Meeeee, M.; Meeeeeee, M., Meeeee M. Meee., Meee. M, (8888) 88, 8888. |
[188] | Meeeee, M.; Meeeeee, M.; Meeee, M.; Meeee, M.; Meeeee-Meeeeee, M.; Meeeeee, M.; Meeeeeeee, M.; Meeeeeee, M.; Meeeeee, M., Meeeee. Mee. Meee. Meee., (8888) 8, 8888. |
[189] | Meeeee, M. M.; Meeee, M. M.; Meeeeeeeeeee, M., Meeeee M. Meee., Meee. M, (8888) 88, 888. |
[190] | Meeee, M. M.; Meeeeee, M. M., Meeeee M. Meee., Meee. M, (8888) 88, 88. |
[191] | Meee, M.; Meeeeee, M.; Meeeeeee, M.; Meeeeee, M., Meeeeeeeeeee, (8888) 88, 888. |
[192] | Meeeeeeee, M.; Meeeeee, M.; Meeeeee, M.; Meeeeee, M., Meee. Mee. Meee. Meee., (8888) 888, 888. |
[193] | Meeeeeeeeeeeee, M. M.; Meeeeeee, M. M., Meeee. Meeeee., (8888) 88, 888. |
[194] | Meeee, M.; Meeeee, M.; Meeee, M. M., M. Meeeee Meee. Mee., (8888) 88, 888. |
[195] | Meeee, M. M.; Meee, M. M., M. Meee. Mee., (8888), 88. |
[196] | Meeeeee, M.; Meeee, M. M. M.; Meeeee, M. M., Meeeeeeeeee Meee., (8888) 88, 8888. |
[197] | Mee, M.; Meeeeeee, M., M. Meeeeeeeee. Meee., (8888) 88, 888. |
[198] | Meeeeeeeee, M.; Meeeee, M.; Meeeeeeee, M.; Meeeeee, M.; Meeeeee, M., M. Meeeeeeeee. Meee., (8888) 88, 8888. |
[199] | Meeee, M.; Meeeeeee, M., Meee. Mee. Meee. Meee., (8888) 888, 888. |
[200] | Meeeeeeeee-Meeeeee, M.; Meeeeeeee, M.; Meeee, M.; Meeeeeeeee, M., Meeeee. Mee. Meee. Meee., (8888) 8, 8888. |
[201] | Meeeeeee, M. M.; Meeee, M. M.; Meeeeeee, M. M., Meeeee M. Meee., Meee. M, (8888) 88, 888. |
[202] | Meeeeee, M.; Meeee, M. M. M.; Meeeee, M. M., M. Meee. Mee., Meeeee Meeee. 8, (8888), 888. |
[203] | Meeeeeeee, M.; Meeeeeee, M. M., M. Meee. Mee., (8888), 8888. |
[204] | Meeeeeeeee, M.; Meeeeeeeee, M. M., M. Me. Meee. Mee., (8888) 88, 8888. |
[205] | Meeeeee, M. M., Meeeeeeeeee, (8888) 88, 8888. |
[206] | Meeeeeeee, M. M.; Meeee, M. M., Meeeeeeee, (8888), 88. |
[207] | Meeee, M.; Meeeeeee, M. M., M. Me. Meee. Mee., (8888) 88, 888. |
[208] | Meeee, M. M.; Meeeeeee, M.; Meeee, M. M., Meeeee M. Meee., (8888) 8, 88. |
[209] | Meeeeeeeee, M.; Meeeeee, M.; Mee, M., Meeeeeeeeee, (8888) 88, 8888. |
Meeeeee Meeeeeeeeee
- 8.Meeeee-Meee, (8888) 8/8, 888.
- 8.Meeeee-Meee, (8888) 8/8, 888.