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Glass, R. S., Science of Synthesis, (2005) 22, 81.
Chlorosulfines 13 can be prepared by the oxidation of thioacyl chlorides (Scheme 10).[20,21] Chlorosulfines decompose on storage at room temperature and must be protected from water and light but can be stored at −5°C for a few weeks with minimal decomposition.
Meeeee 88 Meeeeeeee ee Meeeeeee Meeeeeeee[88,88]
Meeeeeeeeeee Meeeeeeee
eee - eee eeeee-[Meeeee(eeeeeeee)eeeeee]eeeeeee (88, M8 = Me):[88]
Me e eeee ee eeeeeee eeeeeeeee MeMMMe (8.88 e, 88 eeee) ee MMMe8 (888 eM) eee eeeee eeeeeeeeeeeeeeeeee eeee (88.88 e, 88 eeee) ee Me8M (888 eM) ee 8°M eeee 8 e. Meeee eee eeeeeeee eee eeeeeeee, eeeeeeee eee eeeeeeeee eee 8 e. Mee eeeeeeeeeeee eeeeeeee eeee eee eeeeeee ee eeeeeeeeee. Mee eeeeeeee eeee eeee eeeeeeeeeeeee e eeeeeee eeee eeeee eee eeeee eeeeeee eee eeeeeeee ee eeeeeeeeee eeee MMMe8. Meee eeeeeee eee eeeeeeeeeeeeeee [eeeeee eee, eeeeeeeee eeeee (ee 88–88°M)/eeeeeee (MMMMMMM: eeeeeeeeee) 8:8] ee eeee eee eeee eeeee-eeeeeee; eeeee: 8.88 e (88%); eee eeee eeeee eeeeeeeeeeeeeee (eeeeee eee, eeeeeee) ee eeee eee eee-eeeeeee ee eeeeee eeeeeeee; eeeee: 8.88 e (88%); ee 88–88°M.
References
| [20] | Meeeeeeeee, M.; Meeee, M.; Meeeeeee, M., Meee. Meee. Meee. Meee-Mee, (8888) 88, 888. |
| [21] | Meeeeeee, M. M.; Meeee, M. M., M. Mee. Meee., (8888) 88, 8888. |
Meeeeee Meeeeeeeeee
- 8.Meeeee-Meee, (8888) M 8-8, 888.
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